Information card for entry 4335188

Structure parameters

• Formula: C27 H33.5 F12 N6.5 O0.5 P Ru Sb2
• Calculated formula: C27 H33.5 F12 N6.5 O0.5 P Ru Sb2
• Title of publication: Tri(pyridylmethyl)phosphine: The Elusive Congener of TPA Shows Surprisingly Different Coordination Behavior
• Authors of publication: Christopher J. Whiteoak; James D. Nobbs; Evgeny Kiryushchenkov; Sandro Pagano; Andrew J.P. White; George J.P. Britovsek
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 7000 - 7009
• a: 10.7301 ± 0.0003 Å
• b: 37.0357 ± 0.0011 Å
• c: 20.8357 ± 0.001 Å
• α: 90°
• β: 101.078 ± 0.004°
• γ: 90°
• Cell volume: 8125.8 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0922
• Residual factor for significantly intense reflections: 0.0737
• Weighted residual factors for significantly intense reflections: 0.22
• Weighted residual factors for all reflections included in the refinement: 0.2349
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No