Information card for entry 4335363

Structure parameters

• Formula: C30 H68 N6 O14 P2 Pd6 S2
• Calculated formula: C30 H68 N6 O14 P2 Pd6 S2
• Title of publication: Facile Formation of Stable Tris(imido)phosphate Trianions as Their Tri- and Hexanuclear Pd(II) Complexes in Protic Solvents
• Authors of publication: Arvind K. Gupta; S. Arun Dixith Reddy; Ramamoorthy Boomishankar
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 7608 - 7614
• a: 24.812 ± 0.003 Å
• b: 9.7381 ± 0.0014 Å
• c: 23.628 ± 0.003 Å
• α: 90°
• β: 120.349 ± 0.002°
• γ: 90°
• Cell volume: 4926.7 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0541
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.081
• Weighted residual factors for all reflections included in the refinement: 0.0887
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No