Information card for entry 4335364

Structure parameters

• Formula: C42 H85 N6 O9 P Pd3
• Calculated formula: C42 H81 N6 O9.025 P Pd3
• Title of publication: Facile Formation of Stable Tris(imido)phosphate Trianions as Their Tri- and Hexanuclear Pd(II) Complexes in Protic Solvents
• Authors of publication: Arvind K. Gupta; S. Arun Dixith Reddy; Ramamoorthy Boomishankar
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 7608 - 7614
• a: 17.0471 ± 0.0016 Å
• b: 17.0471 ± 0.0016 Å
• c: 22.921 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5768.5 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 165
• Hermann-Mauguin space group symbol: P -3 c 1
• Hall space group symbol: -P 3 2"c
• Residual factor for all reflections: 0.1243
• Residual factor for significantly intense reflections: 0.0614
• Weighted residual factors for significantly intense reflections: 0.1843
• Weighted residual factors for all reflections included in the refinement: 0.225
• Goodness-of-fit parameter for all reflections included in the refinement: 0.88
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No