Information card for entry 4335573

Structure parameters

• Formula: Ge4 H154 K26 Ni10 O210 W34
• Calculated formula: Ge4 K18.2 Ni10 O203 W34
• Title of publication: Synthesis, Magnetism, and Electrochemistry of the Ni14- and Ni5-Containing Heteropolytungstates [Ni14(OH)6(H2O)10(HPO4)4(P2W15O56)4]34- and [Ni5(OH)4(H2O)4(β-GeW9O34)(β-GeW8O30(OH))]13-
• Authors of publication: Masooma Ibrahim; Yixian Xiang; Bassem S. Bassil; Yanhua Lan; Annie K. Powell; Pedro de Oliveira; Bineta Keita; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 8399 - 8408
• a: 18.4924 ± 0.0004 Å
• b: 21.8208 ± 0.0004 Å
• c: 25.2971 ± 0.0006 Å
• α: 81.747 ± 0.001°
• β: 73.893 ± 0.001°
• γ: 85.101 ± 0.001°
• Cell volume: 9694.4 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0879
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1331
• Weighted residual factors for all reflections included in the refinement: 0.1566
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No