Information card for entry 4335903

Structure parameters

• Formula: C37 H23 D12 F9 I N5 Zr
• Calculated formula: C37 H23 D12 F9 I N5 Zr
• Title of publication: Zirconium Complexes Supported by an N-Perfluoro-Arylated Diamidopyridyl Ligand: Synthesis of Hydrazinediido Complexes
• Authors of publication: Solveig A. Scholl; Gudrun T. Plundrich; Hubert Wadepohl; Lutz H. Gade
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 10158 - 10166
• a: 8.33711 ± 0.00008 Å
• b: 23.5742 ± 0.0002 Å
• c: 9.73406 ± 0.0001 Å
• α: 90°
• β: 109.294 ± 0.0011°
• γ: 90°
• Cell volume: 1805.69 ± 0.03 ų
• Cell temperature: 110 ± 0.1 K
• Ambient diffraction temperature: 110 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.0221
• Weighted residual factors for significantly intense reflections: 0.0432
• Weighted residual factors for all reflections included in the refinement: 0.0458
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No