Crystallography Open Database

Information card for entry 4335904

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Coordinates	4335904.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H23 Cl F9 N5 Zr
Calculated formula	C25 H23 Cl F9 N5 Zr
Title of publication	Zirconium Complexes Supported by an N-Perfluoro-Arylated Diamidopyridyl Ligand: Synthesis of Hydrazinediido Complexes
Authors of publication	Solveig A. Scholl; Gudrun T. Plundrich; Hubert Wadepohl; Lutz H. Gade
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	10158 - 10166
a	8.33527 ± 0.00004 Å
b	18.16024 ± 0.00009 Å
c	9.30851 ± 0.00005 Å
α	90°
β	110.913 ± 0.0006°
γ	90°
Cell volume	1316.21 ± 0.013 Å³
Cell temperature	114.95 ± 0.18 K
Ambient diffraction temperature	114.95 ± 0.18 K
Number of distinct elements	6
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0206
Residual factor for significantly intense reflections	0.0189
Weighted residual factors for significantly intense reflections	0.0507
Weighted residual factors for all reflections included in the refinement	0.0517
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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