Information card for entry 4336289

Structure parameters

• Chemical name: 1,3-dichloro-2,4-bis(bis-trimethylsilylamino)-cyclo-1,3-diphospha-2,4-diazane
• Formula: C12 H36 Cl2 N4 P2 Si4
• Calculated formula: C12 H36 Cl2 N4 P2 Si4
• Title of publication: Synthesis of 1,3-Dichloro-cyclo-1,3-diphosphadiazanes from Silylated Amino(dichloro)phosphanes
• Authors of publication: Axel Schulz; Alexander Villinger; Andrea Westenkirchner
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 11457 - 11468
• a: 13.0246 ± 0.0005 Å
• b: 15.6553 ± 0.0006 Å
• c: 13.0864 ± 0.0005 Å
• α: 90°
• β: 91.561 ± 0.002°
• γ: 90°
• Cell volume: 2667.38 ± 0.18 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0759
• Residual factor for significantly intense reflections: 0.0492
• Weighted residual factors for significantly intense reflections: 0.1237
• Weighted residual factors for all reflections included in the refinement: 0.1344
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No