Information card for entry 4336290

Structure parameters

• Chemical name: 1,3-bis(1,1,1,3,3,3-hexafluoro-2-propoxy)-2,4-bis(trimethylsilyl)-cyclo- 1,3-diphospha-2,4-diazane
• Formula: C12 H20 F12 N2 O2 P2 Si2
• Calculated formula: C12 H20 F12 N2 O2 P2 Si2
• Title of publication: Synthesis of 1,3-Dichloro-cyclo-1,3-diphosphadiazanes from Silylated Amino(dichloro)phosphanes
• Authors of publication: Axel Schulz; Alexander Villinger; Andrea Westenkirchner
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 11457 - 11468
• a: 20.253 ± 0.0016 Å
• b: 8.7053 ± 0.0007 Å
• c: 13.4567 ± 0.0011 Å
• α: 90°
• β: 96.091 ± 0.004°
• γ: 90°
• Cell volume: 2359.1 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0779
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0879
• Weighted residual factors for all reflections included in the refinement: 0.0971
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No