Information card for entry 4336681

Structure parameters

• Formula: C19 H31 Fe0.5 O2
• Calculated formula: C19 H31 Fe0.5 O2
• Title of publication: Reductive Coupling of Azides Mediated by an Iron(II) Bis(alkoxide) Complex
• Authors of publication: James A. Bellow; Philip D. Martin; Richard L. Lord; Stanislav Groysman
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 12335 - 12337
• a: 21.0091 ± 0.0013 Å
• b: 36.694 ± 0.002 Å
• c: 9.3124 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7179 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0369
• Residual factor for significantly intense reflections: 0.0316
• Weighted residual factors for significantly intense reflections: 0.0781
• Weighted residual factors for all reflections included in the refinement: 0.0799
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No