Information card for entry 4336682

Structure parameters

• Formula: C45 H77 Fe N3 O2
• Calculated formula: C45.5 H61 Fe N3 O2
• Title of publication: Reductive Coupling of Azides Mediated by an Iron(II) Bis(alkoxide) Complex
• Authors of publication: James A. Bellow; Philip D. Martin; Richard L. Lord; Stanislav Groysman
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 12335 - 12337
• a: 12.9324 ± 0.0006 Å
• b: 12.933 ± 0.0006 Å
• c: 14.1689 ± 0.0007 Å
• α: 93.36 ± 0.002°
• β: 93.147 ± 0.002°
• γ: 115.75 ± 0.002°
• Cell volume: 2122.29 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0685
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1488
• Weighted residual factors for all reflections included in the refinement: 0.16
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No