Information card for entry 4337960

Structure parameters

• Formula: C12 H28 Cl6 Ga N3 P2
• Calculated formula: C12 H28 Cl6 Ga N3 P2
• Title of publication: Azidophosphenium Cations: Versatile Reagents in Inorganic Synthesis.
• Authors of publication: Hering, Christian; Hertrich, Maximilian; Schulz, Axel; Villinger, Alexander
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 7
• Pages of publication: 3880
• a: 13.0816 ± 0.0003 Å
• b: 11.9343 ± 0.0003 Å
• c: 31.5103 ± 0.0008 Å
• α: 90°
• β: 90.949 ± 0.001°
• γ: 90°
• Cell volume: 4918.7 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1181
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.0719
• Weighted residual factors for all reflections included in the refinement: 0.0889
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No