Information card for entry 4337961

Structure parameters

• Formula: C12 H32 Cl6 Ga N3 P2 Si2
• Calculated formula: C12 H32 Cl6 Ga N3 P2 Si2
• Title of publication: Azidophosphenium Cations: Versatile Reagents in Inorganic Synthesis.
• Authors of publication: Hering, Christian; Hertrich, Maximilian; Schulz, Axel; Villinger, Alexander
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 7
• Pages of publication: 3880
• a: 9.08 ± 0.0007 Å
• b: 26.0437 ± 0.0018 Å
• c: 12.1092 ± 0.0009 Å
• α: 90°
• β: 95.938 ± 0.003°
• γ: 90°
• Cell volume: 2848.2 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.103
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.0898
• Weighted residual factors for all reflections included in the refinement: 0.105
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No