Information card for entry 4338137

Structure parameters

• Formula: C15 H41 K N4 Sn
• Calculated formula: C15 H41 K N4 Sn
• Title of publication: K-H3C and K-Sn Interactions in Potassium Trimethylstannyl Complexes: A Structural, Mechanochemical, and NMR Study.
• Authors of publication: Kleeberg, Christian; Grunenberg, Jörg; Xie, Xiulan
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 9
• Pages of publication: 4400 - 4410
• a: 14.6515 ± 0.001 Å
• b: 22.3453 ± 0.0016 Å
• c: 14.4641 ± 0.001 Å
• α: 90°
• β: 99.96 ± 0.005°
• γ: 90°
• Cell volume: 4664.1 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0795
• Residual factor for significantly intense reflections: 0.0524
• Weighted residual factors for significantly intense reflections: 0.1393
• Weighted residual factors for all reflections included in the refinement: 0.1584
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No