Information card for entry 4338138

Structure parameters

• Formula: C19 H41 K O8 Sn
• Calculated formula: C19 H41 K O8 Sn
• Title of publication: K-H3C and K-Sn Interactions in Potassium Trimethylstannyl Complexes: A Structural, Mechanochemical, and NMR Study.
• Authors of publication: Kleeberg, Christian; Grunenberg, Jörg; Xie, Xiulan
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 9
• Pages of publication: 4400 - 4410
• a: 7.6217 ± 0.0012 Å
• b: 21.232 ± 0.004 Å
• c: 8.1478 ± 0.0013 Å
• α: 90°
• β: 99.082 ± 0.016°
• γ: 90°
• Cell volume: 1302 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.1024
• Residual factor for significantly intense reflections: 0.0641
• Weighted residual factors for significantly intense reflections: 0.1339
• Weighted residual factors for all reflections included in the refinement: 0.143
• Goodness-of-fit parameter for all reflections included in the refinement: 0.946
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No