Information card for entry 4338351

Structure parameters

• Formula: C42 H34 Cl4 O32 P4 Re4
• Calculated formula: C42 H28 Cl4 O32 P4 Re4
• Title of publication: New class of phosphine oxide donor-based supramolecular coordination complexes from an in situ phosphine oxidation reaction or phosphine oxide ligands.
• Authors of publication: Shankar, Bhaskaran; Elumalai, Palani; Shanmugam, Ramasamy; Singh, Virender; Masram, Dhanraj T.; Sathiyendiran, Malaichamy
• Journal of publication: Inorganic chemistry
• Year of publication: 2013
• Journal volume: 52
• Journal issue: 18
• Pages of publication: 10217 - 10219
• a: 10.0213 ± 0.0004 Å
• b: 12.6007 ± 0.0004 Å
• c: 12.9155 ± 0.0005 Å
• α: 99.129 ± 0.003°
• β: 107.872 ± 0.004°
• γ: 99.948 ± 0.003°
• Cell volume: 1489.39 ± 0.11 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.069
• Weighted residual factors for all reflections included in the refinement: 0.0717
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No