Crystallography Open Database

Information card for entry 4338352

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Coordinates	4338352.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H103 Mo24 N4 Na5 O138 P12
Calculated formula	C12 H24 Mo24 N4 Na5 O138 P12
Title of publication	A crown-shaped 24-molybdate cluster constructed by organotriphosphonate ligand.
Authors of publication	Yang, Lu; Ma, Pengtao; Zhou, Zhen; Wang, Jingping; Niu, Jingyang
Journal of publication	Inorganic chemistry
Year of publication	2013
Journal volume	52
Journal issue	15
Pages of publication	8285 - 8287
a	11.8607 ± 0.0016 Å
b	50.637 ± 0.007 Å
c	61.215 ± 0.008 Å
α	90°
β	90°
γ	90°
Cell volume	36765 ± 9 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	70
Hermann-Mauguin space group symbol	F d d d :2
Hall space group symbol	-F 2uv 2vw
Residual factor for all reflections	0.0767
Residual factor for significantly intense reflections	0.0592
Weighted residual factors for significantly intense reflections	0.1756
Weighted residual factors for all reflections included in the refinement	0.1908
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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