Information card for entry 4339111

Structure parameters

• Chemical name: (K-crown)2[CH2=CH-Ge9-CHCH2] en
• Formula: C30 H62 Ge9 K2 N2 O12
• Calculated formula: C30 H62 Ge9 K2 N2 O12
• Title of publication: Organo-Zintl clusters soluble in conventional organic solvents: setting the stage for organo-Zintl cluster chemistry.
• Authors of publication: Hull, Michael W.; Sevov, Slavi C.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 26
• Pages of publication: 10953 - 10955
• a: 10.9474 ± 0.0004 Å
• b: 14.3863 ± 0.0005 Å
• c: 16.2272 ± 0.0006 Å
• α: 85.946 ± 0.002°
• β: 71.136 ± 0.002°
• γ: 89.264 ± 0.002°
• Cell volume: 2412.21 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0354
• Residual factor for significantly intense reflections: 0.0236
• Weighted residual factors for significantly intense reflections: 0.054
• Weighted residual factors for all reflections included in the refinement: 0.0591
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No