Information card for entry 4339112

Structure parameters

• Chemical name: (Me4N)2[CH2=CH-Ge9-CHCH2] 0.5en
• Formula: C13 H34 Ge9 N3
• Calculated formula: C13 H34 Ge9 N3
• Title of publication: Organo-Zintl clusters soluble in conventional organic solvents: setting the stage for organo-Zintl cluster chemistry.
• Authors of publication: Hull, Michael W.; Sevov, Slavi C.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 26
• Pages of publication: 10953 - 10955
• a: 30.2772 ± 0.0015 Å
• b: 13.3218 ± 0.0007 Å
• c: 15.4229 ± 0.0008 Å
• α: 90°
• β: 118.552 ± 0.003°
• γ: 90°
• Cell volume: 5464.2 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0462
• Residual factor for significantly intense reflections: 0.0296
• Weighted residual factors for significantly intense reflections: 0.0729
• Weighted residual factors for all reflections included in the refinement: 0.0764
• Goodness-of-fit parameter for all reflections included in the refinement: 1.158
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No