Information card for entry 4339394

Structure parameters

• Formula: C70 H83 Cl2 Li3 O11.5 Pr Si4
• Calculated formula: C70 H83 Cl2 Li3 O11.5 Pr Si4
• Title of publication: Structural varieties in heterobimetallic lanthanide disiloxanediolates: "inorganic metallocenes" versus in-plane metallacrowns.
• Authors of publication: Giessmann, Stephan; Blaurock, Steffen; Lorenz, Volker; Edelmann, Frank T.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 24
• Pages of publication: 10383 - 10389
• a: 14.0067 ± 0.0002 Å
• b: 22.8399 ± 0.0004 Å
• c: 23.0701 ± 0.0004 Å
• α: 90°
• β: 90.64°
• γ: 90°
• Cell volume: 7379.9 ± 0.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.1162
• Weighted residual factors for all reflections included in the refinement: 0.1246
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No