Information card for entry 4339395

Structure parameters

• Formula: C60 H69.29 Cl Li2 O11.64 Sc Si4
• Calculated formula: C60 H69.196 Cl Li2 O11.598 Sc Si4
• Title of publication: Structural varieties in heterobimetallic lanthanide disiloxanediolates: "inorganic metallocenes" versus in-plane metallacrowns.
• Authors of publication: Giessmann, Stephan; Blaurock, Steffen; Lorenz, Volker; Edelmann, Frank T.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 24
• Pages of publication: 10383 - 10389
• a: 17.0335 ± 0.0019 Å
• b: 20.649 ± 0.002 Å
• c: 35.785 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12586 ± 2 ų
• Cell temperature: 210 ± 2 K
• Ambient diffraction temperature: 210 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0775
• Residual factor for significantly intense reflections: 0.0528
• Weighted residual factors for significantly intense reflections: 0.1263
• Weighted residual factors for all reflections included in the refinement: 0.14
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No