Information card for entry 4339582

Structure parameters

• Formula: C27 H42 Cl2 N3 O8 Rh
• Calculated formula: C27 H41.697 Cl2 N3 O8 Rh
• Title of publication: On the reactivity toward ketones of new methyl amino complexes of Rh(III) and Ag(I). Synthesis of ortho-rhodiated acetophenone methyl imine complexes.
• Authors of publication: Vicente, José; Chicote, María Teresa; Vicente-Hernandez, Inmaculada; Bautista, Delia
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 21
• Pages of publication: 8939 - 8949
• a: 11.339 ± 0.0005 Å
• b: 15.8885 ± 0.0006 Å
• c: 17.0075 ± 0.0007 Å
• α: 90°
• β: 96.14 ± 0.002°
• γ: 90°
• Cell volume: 3046.5 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0399
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0744
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No