Information card for entry 4339583

Structure parameters

• Formula: C22 H36 Cl2 D6 N3 O9 Rh
• Calculated formula: C22 H42 Cl2 N3 O9 Rh
• Title of publication: On the reactivity toward ketones of new methyl amino complexes of Rh(III) and Ag(I). Synthesis of ortho-rhodiated acetophenone methyl imine complexes.
• Authors of publication: Vicente, José; Chicote, María Teresa; Vicente-Hernandez, Inmaculada; Bautista, Delia
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 21
• Pages of publication: 8939 - 8949
• a: 10.38 ± 0.0005 Å
• b: 11.1724 ± 0.0005 Å
• c: 13.4906 ± 0.0006 Å
• α: 68.798 ± 0.002°
• β: 86.115 ± 0.002°
• γ: 82.602 ± 0.002°
• Cell volume: 1446.08 ± 0.12 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0295
• Residual factor for significantly intense reflections: 0.0291
• Weighted residual factors for significantly intense reflections: 0.0716
• Weighted residual factors for all reflections included in the refinement: 0.0719
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No