Information card for entry 4341636

Structure parameters

• Formula: C9 H74 Co2 K6 N3.6 Na6 O108 Sb2 W20
• Calculated formula: C9.5 H5.7 Co2.018 K3.8 N3.8 Na5.8 O105.7 Sb2 W19.982
• Title of publication: Functionalization of krebs-type polyoxometalates with n,o-chelating ligands: a systematic study.
• Authors of publication: Artetxe, Beñat; Reinoso, Santiago; San Felices, Leire; Vitoria, Pablo; Pache, Aroa; Martín-Caballero, Jagoba; Gutiérrez-Zorrilla, Juan M
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 1
• Pages of publication: 241 - 252
• a: 12.2033 ± 0.0004 Å
• b: 15.0427 ± 0.0004 Å
• c: 15.8975 ± 0.0005 Å
• α: 73.22 ± 0.002°
• β: 78.478 ± 0.003°
• γ: 67.035 ± 0.003°
• Cell volume: 2560.02 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0405
• Residual factor for significantly intense reflections: 0.0353
• Weighted residual factors for significantly intense reflections: 0.0801
• Weighted residual factors for all reflections included in the refinement: 0.0831
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No