Information card for entry 4341637

Structure parameters

• Formula: C8 H74.4 K6 N3.2 Na6 O109 Sb2 W20.4 Zn1.6
• Calculated formula: C8.35 H5.01 K4.8 N3.34 Na2 O103.67 Sb2 W20.33 Zn1.67
• Title of publication: Functionalization of krebs-type polyoxometalates with n,o-chelating ligands: a systematic study.
• Authors of publication: Artetxe, Beñat; Reinoso, Santiago; San Felices, Leire; Vitoria, Pablo; Pache, Aroa; Martín-Caballero, Jagoba; Gutiérrez-Zorrilla, Juan M
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 1
• Pages of publication: 241 - 252
• a: 12.2715 ± 0.0003 Å
• b: 15.9492 ± 0.0006 Å
• c: 16.0131 ± 0.0005 Å
• α: 65.534 ± 0.003°
• β: 67.844 ± 0.003°
• γ: 78.232 ± 0.002°
• Cell volume: 2637.79 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0425
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0943
• Weighted residual factors for all reflections included in the refinement: 0.0969
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No