Crystallography Open Database

Information card for entry 4342280

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Coordinates	4342280.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H77 Cl2 F Ge N6
Calculated formula	C60 H77 Cl2 F Ge N6
Title of publication	Contrasting reactivities of silicon and germanium complexes supported by an N-heterocyclic guanidine ligand.
Authors of publication	Lui, Melanie W.; Merten, Christian; Ferguson, Michael J.; McDonald, Robert; Xu, Yunjie; Rivard, Eric
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	4
Pages of publication	2040 - 2049
a	19.1837 ± 0.0003 Å
b	12.563 ± 0.0002 Å
c	25.6436 ± 0.0004 Å
α	90°
β	110.829 ± 0.0005°
γ	90°
Cell volume	5776.33 ± 0.16 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0397
Residual factor for significantly intense reflections	0.0373
Weighted residual factors for significantly intense reflections	0.1029
Weighted residual factors for all reflections included in the refinement	0.1056
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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