Information card for entry 4342281

Structure parameters

• Formula: C54 H72 Cl0.09 Ge N6
• Calculated formula: C54 H72 Cl0.09 Ge N6
• Title of publication: Contrasting reactivities of silicon and germanium complexes supported by an N-heterocyclic guanidine ligand.
• Authors of publication: Lui, Melanie W.; Merten, Christian; Ferguson, Michael J.; McDonald, Robert; Xu, Yunjie; Rivard, Eric
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 4
• Pages of publication: 2040 - 2049
• a: 11.8062 ± 0.0003 Å
• b: 19.8956 ± 0.0005 Å
• c: 21.8851 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5140.6 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0464
• Residual factor for significantly intense reflections: 0.0355
• Weighted residual factors for significantly intense reflections: 0.0926
• Weighted residual factors for all reflections included in the refinement: 0.0996
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No