Information card for entry 4342307

Structure parameters

• Formula: C25 H28 Al0.17 Pb0.83
• Calculated formula: C25 H28 Al0.17 Pb0.83
• Title of publication: Reaction of a germylene, stannylene, or plumbylene with trimethylaluminum and trimethylgallium: insertion into Al-C or ga-C bonds, a reversible metal-carbon insertion equilibrium, and a new route to diplumbenes.
• Authors of publication: Erickson, Jeremy D.; Fettinger, James C.; Power, Philip P.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 4
• Pages of publication: 1940 - 1948
• a: 11.508 ± 0.0005 Å
• b: 12.5011 ± 0.0006 Å
• c: 14.8554 ± 0.0007 Å
• α: 90°
• β: 93.2786 ± 0.0016°
• γ: 90°
• Cell volume: 2133.64 ± 0.17 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0298
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0735
• Weighted residual factors for all reflections included in the refinement: 0.0738
• Goodness-of-fit parameter for all reflections included in the refinement: 1.229
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No