Crystallography Open Database

Information card for entry 4343299

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Coordinates	4343299.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C63 H47 B F25 N2 Rh
Calculated formula	C63 H47 B F25 N2 Rh
Title of publication	Synthesis and Reactivity toward H2 of (η(5)-C5Me5)Rh(III) Complexes with Bulky Aminopyridinate Ligands.
Authors of publication	Zamorano, Ana; Rendón, Nuria; Valpuesta, José E V; Álvarez, Eleuterio; Carmona, Ernesto
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	13
Pages of publication	6573 - 6581
a	22.0782 ± 0.0008 Å
b	12.7398 ± 0.0004 Å
c	22.0446 ± 0.0008 Å
α	90°
β	97.843 ± 0.001°
γ	90°
Cell volume	6142.5 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0397
Residual factor for significantly intense reflections	0.0335
Weighted residual factors for significantly intense reflections	0.0829
Weighted residual factors for all reflections included in the refinement	0.0855
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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