Information card for entry 4343988

Structure parameters

• Formula: C32 H45.9 Cl2 N6 O12.45 V2
• Calculated formula: C32 H30 Cl2 N6 O12.456 V2
• Title of publication: Aerial Oxidation of a V(IV)-Iminopyridine Hydroquinonate Complex: A Trap for the V(IV)-Semiquinonate Radical Intermediate.
• Authors of publication: Stylianou, Marios; Drouza, Chryssoula; Giapintzakis, John; Athanasopoulos, Georgios I.; Keramidas, Anastasios D.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 15
• Pages of publication: 7218 - 7229
• a: 24.974 ± 0.0011 Å
• b: 24.974 ± 0.0014 Å
• c: 17.5048 ± 0.0006 Å
• α: 90 ± 0.004°
• β: 90 ± 0.003°
• γ: 120 ± 0.005°
• Cell volume: 9455.1 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1489
• Weighted residual factors for all reflections included in the refinement: 0.1563
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No