Information card for entry 4344046

Structure parameters

• Common name: (Kcrypt)2{(Ge9R3)PdGe9R3)}.2MeCN
• Formula: C47 H120 Ge9 K N3 O6 Pd0.5 Si12
• Calculated formula: C47 H120 Ge9 K N3 O6 Pd0.5 Si12
• Title of publication: Coordination of Tri-Substituted Nona-Germanium Clusters to Cu(I) and Pd(0).
• Authors of publication: Li, Feng; Sevov, Slavi C.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 16
• Pages of publication: 8121 - 8125
• a: 15.5519 ± 0.0012 Å
• b: 16.8841 ± 0.0014 Å
• c: 18.1601 ± 0.0015 Å
• α: 64.778 ± 0.002°
• β: 79.495 ± 0.003°
• γ: 89.554 ± 0.003°
• Cell volume: 4228.4 ± 0.6 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0496
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0692
• Weighted residual factors for all reflections included in the refinement: 0.0775
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No