Information card for entry 4344047

Structure parameters

• Common name: (Ge9Si(SiMe3)3)Cu(Ge9Si(SiMe3)3)CuPPh3 2.5hex
• Formula: C29 H70.67 Cu0.67 Ge6 P0.33 Si8
• Calculated formula: C29 H70.6667 Cu0.666667 Ge6 P0.333333 Si8
• Title of publication: Coordination of Tri-Substituted Nona-Germanium Clusters to Cu(I) and Pd(0).
• Authors of publication: Li, Feng; Sevov, Slavi C.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 16
• Pages of publication: 8121 - 8125
• a: 38.399 ± 0.003 Å
• b: 27.38 ± 0.003 Å
• c: 30.128 ± 0.002 Å
• α: 90°
• β: 91.359 ± 0.002°
• γ: 90°
• Cell volume: 31667 ± 5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0647
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.0937
• Weighted residual factors for all reflections included in the refinement: 0.1054
• Goodness-of-fit parameter for all reflections included in the refinement: 1.118
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No