Information card for entry 4344934

Structure parameters

• Formula: C8 H16 N8 Ni2 O8 W
• Calculated formula: C8 H16 N8 Ni2 O8 W
• Title of publication: Dehydration of Octacyanido-Bridged Ni(II)-W(IV) Framework toward Negative Thermal Expansion and Magneto-Colorimetric Switching.
• Authors of publication: Reczyński, Mateusz; Chorazy, Szymon; Nowicka, Beata; Sieklucka, Barbara; Ohkoshi, Shin-Ichi
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• a: 11.6752 ± 0.0006 Å
• b: 11.6752 ± 0.0006 Å
• c: 12.8954 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1757.78 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 87
• Hermann-Mauguin space group symbol: I 4/m
• Hall space group symbol: -I 4
• Residual factor for all reflections: 0.0199
• Residual factor for significantly intense reflections: 0.0194
• Weighted residual factors for significantly intense reflections: 0.0331
• Weighted residual factors for all reflections included in the refinement: 0.0332
• Goodness-of-fit parameter for all reflections included in the refinement: 1.464
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No