Information card for entry 4344935

Structure parameters

• Formula: C4 N4 Ni W0.5
• Calculated formula: C4 N4 Ni W0.5
• Title of publication: Dehydration of Octacyanido-Bridged Ni(II)-W(IV) Framework toward Negative Thermal Expansion and Magneto-Colorimetric Switching.
• Authors of publication: Reczyński, Mateusz; Chorazy, Szymon; Nowicka, Beata; Sieklucka, Barbara; Ohkoshi, Shin-Ichi
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• a: 10.9485 ± 0.0013 Å
• b: 10.9485 ± 0.0013 Å
• c: 12.7277 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1525.7 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 140
• Hermann-Mauguin space group symbol: I 4/m c m
• Hall space group symbol: -I 4 2c
• Residual factor for all reflections: 0.04
• Residual factor for significantly intense reflections: 0.04
• Weighted residual factors for significantly intense reflections: 0.0873
• Weighted residual factors for all reflections included in the refinement: 0.0873
• Goodness-of-fit parameter for all reflections included in the refinement: 1.262
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No