Information card for entry 4346198

Structure parameters

• Formula: C62 H43 B2 F42 N9 Zn
• Calculated formula: C62 H43 B2 F42 N9 Zn
• Title of publication: Zinc-Mediated Carbene Insertion to C-Cl Bonds of Chloromethanes and Isolable Zinc(II) Isocyanide Adducts.
• Authors of publication: Kulkarni, Naveen V.; Das, Animesh; Jayaratna, Naleen B.; Yousufuddin, Muhammed; Dias, H. V. Rasika
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 11
• Pages of publication: 5151 - 5153
• a: 24.2453 ± 0.0016 Å
• b: 15.649 ± 0.002 Å
• c: 20.561 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7801.1 ± 1.6 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200.01 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0981
• Residual factor for significantly intense reflections: 0.0726
• Weighted residual factors for significantly intense reflections: 0.1942
• Weighted residual factors for all reflections included in the refinement: 0.2125
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No