Information card for entry 4505909

Structure parameters

• Chemical name: [tris(2,2'-bipyridine-4,4'-diamine)(nitrato)cobalt(II)] nitrate dimethylformamide clathrate
• Formula: C53.5 H71.5 Co2 N24.5 O16.5
• Calculated formula: C53.5 H71.5 Co2 N24.5 O16.5
• Title of publication: Metal Complexes of 2,2′-Bipyridine-4,4′-diamine as Metallo-Tectons for Hydrogen Bonded Networks
• Authors of publication: Rigby, Nicola; Jacobs, Tia; Reddy, Jayarama Prakasha; Hardie, Michaele J.
• Journal of publication: Crystal Growth & Design
• Year of publication: 2012
• Journal volume: 12
• Journal issue: 4
• Pages of publication: 1871
• a: 10.7038 ± 0.0007 Å
• b: 34.312 ± 0.002 Å
• c: 20.5328 ± 0.0011 Å
• α: 90°
• β: 103.605 ± 0.003°
• γ: 90°
• Cell volume: 7329.5 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1356
• Residual factor for significantly intense reflections: 0.0987
• Weighted residual factors for significantly intense reflections: 0.2771
• Weighted residual factors for all reflections included in the refinement: 0.3102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No