Information card for entry 4505910

Structure parameters

• Formula: C54 H44 Ag3.52 Mo8 N14 Na0.48 O27
• Calculated formula: C54 H42 Ag3.516 Mo8 N14 Na0.484 O27
• Title of publication: pH-Controlled Assembly of Two Unusual Entangled Motifs Based on a Tridentate Ligand and Octamolybdate Clusters: 1D + 1D →3D Poly-Pseudorotaxane and 2D →2D →3D Polycatenation
• Authors of publication: Wu, Hua; Yang, Jin; Liu, Ying-Ying; Ma, Jian-Fang
• Journal of publication: Crystal Growth & Design
• Year of publication: 2012
• Journal volume: 12
• Journal issue: 5
• Pages of publication: 2272
• a: 11.0529 ± 0.001 Å
• b: 13.3248 ± 0.001 Å
• c: 13.3632 ± 0.0008 Å
• α: 100.674 ± 0.006°
• β: 94.942 ± 0.006°
• γ: 99.9 ± 0.007°
• Cell volume: 1891 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1131
• Residual factor for significantly intense reflections: 0.0657
• Weighted residual factors for significantly intense reflections: 0.1549
• Weighted residual factors for all reflections included in the refinement: 0.1774
• Goodness-of-fit parameter for all reflections included in the refinement: 0.905
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No