Information card for entry 4516990

Structure parameters

• Formula: C14 H20 Ge O Si2
• Calculated formula: C14 H20 Ge O Si2
• SMILES: [Ge]123[c]4(ccc[cH]14)[Si](O[Si]([c]12ccc[cH]31)(C)C)(C)C
• Title of publication: Synthesis, Structure, and Reactivity of Disiloxa[3]tetrelocenophanes.
• Authors of publication: Wirtz, Lisa; Jourdain, Matthias; Huch, Volker; Zimmer, Michael; Schäfer, André
• Journal of publication: ACS omega
• Year of publication: 2019
• Journal volume: 4
• Journal issue: 19
• Pages of publication: 18355 - 18360
• a: 6.4984 ± 0.0003 Å
• b: 15.098 ± 0.0008 Å
• c: 16.2057 ± 0.0008 Å
• α: 90°
• β: 100.832 ± 0.002°
• γ: 90°
• Cell volume: 1561.66 ± 0.13 ų
• Cell temperature: 152 ± 2 K
• Ambient diffraction temperature: 152 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0353
• Residual factor for significantly intense reflections: 0.0238
• Weighted residual factors for significantly intense reflections: 0.0603
• Weighted residual factors for all reflections included in the refinement: 0.0636
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No