Information card for entry 4516991

Structure parameters

• Formula: C14 H20 O Pb Si2
• Calculated formula: C14 H20 O Pb Si2
• Title of publication: Synthesis, Structure, and Reactivity of Disiloxa[3]tetrelocenophanes.
• Authors of publication: Wirtz, Lisa; Jourdain, Matthias; Huch, Volker; Zimmer, Michael; Schäfer, André
• Journal of publication: ACS omega
• Year of publication: 2019
• Journal volume: 4
• Journal issue: 19
• Pages of publication: 18355 - 18360
• a: 14.6027 ± 0.0005 Å
• b: 21.7849 ± 0.0009 Å
• c: 31.2862 ± 0.0013 Å
• α: 90°
• β: 98.897 ± 0.002°
• γ: 90°
• Cell volume: 9833 ± 0.7 ų
• Cell temperature: 172 ± 2 K
• Ambient diffraction temperature: 172 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0741
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.0782
• Weighted residual factors for all reflections included in the refinement: 0.0898
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No