Information card for entry 4519409

Structure parameters

• Formula: C24 H48 N6 Si2
• Calculated formula: C24 H48 N6 Si2
• Title of publication: Disilanes with Pentacoordinate Si Atoms by Carbon Dioxide Insertion into Aminodisilanes: Syntheses, Molecular Structures, and Dynamic Behavior.
• Authors of publication: Ryll, Christopher; Kraushaar, Konstantin; Wagler, Jörg; Brendler, Erica; Kroke, Edwin
• Journal of publication: ACS omega
• Year of publication: 2022
• Journal volume: 7
• Journal issue: 11
• Pages of publication: 9527 - 9536
• a: 10.0211 ± 0.0005 Å
• b: 17.9266 ± 0.0008 Å
• c: 15.5703 ± 0.0008 Å
• α: 90°
• β: 103.901 ± 0.004°
• γ: 90°
• Cell volume: 2715.2 ± 0.2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0672
• Residual factor for significantly intense reflections: 0.0453
• Weighted residual factors for significantly intense reflections: 0.1176
• Weighted residual factors for all reflections included in the refinement: 0.1313
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No