Information card for entry 4519410

Structure parameters

• Formula: C22 H46 N4 O9 Si2
• Calculated formula: C22 H46 N4 O9 Si2
• Title of publication: Disilanes with Pentacoordinate Si Atoms by Carbon Dioxide Insertion into Aminodisilanes: Syntheses, Molecular Structures, and Dynamic Behavior.
• Authors of publication: Ryll, Christopher; Kraushaar, Konstantin; Wagler, Jörg; Brendler, Erica; Kroke, Edwin
• Journal of publication: ACS omega
• Year of publication: 2022
• Journal volume: 7
• Journal issue: 11
• Pages of publication: 9527 - 9536
• a: 10.2419 ± 0.0007 Å
• b: 11.9781 ± 0.0008 Å
• c: 13.8119 ± 0.0008 Å
• α: 72.61 ± 0.005°
• β: 89.884 ± 0.005°
• γ: 68.752 ± 0.005°
• Cell volume: 1496.25 ± 0.18 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0447
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.099
• Weighted residual factors for all reflections included in the refinement: 0.1035
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No