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Information card for entry 7000149
Preview
Coordinates | 7000149.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H31 F3 N4 Ni P2 |
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Calculated formula | C17 H31 F3 N4 Ni P2 |
SMILES | [Ni]([P](CC)(CC)CC)([P](CC)(CC)CC)(N=N#N)c1nc(F)c(F)cc1F |
Title of publication | C-F Bond activation at Ni(0) and simple reactions of square planar Ni(II) fluoride complexes. |
Authors of publication | Burling, Suzanne; Elliott, Paul I. P.; Jasim, Naser A.; Lindup, Richard J.; McKenna, Jennifer; Perutz, Robin N.; Archibald, Stephen J.; Whitwood, Adrian C. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2005 |
Journal issue | 22 |
Pages of publication | 3686 - 3695 |
a | 9.1396 ± 0.0012 Å |
b | 12.7408 ± 0.0012 Å |
c | 19.819 ± 0.003 Å |
α | 90° |
β | 97.383 ± 0.011° |
γ | 90° |
Cell volume | 2288.7 ± 0.5 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1477 |
Residual factor for significantly intense reflections | 0.045 |
Weighted residual factors for significantly intense reflections | 0.0858 |
Weighted residual factors for all reflections included in the refinement | 0.1082 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.74 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7000149.html
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