Information card for entry 7000150

Structure parameters

• Formula: C19 H33 F4 N Ni O2 P2
• Calculated formula: C19 H33 F4 N Ni O2 P2
• Title of publication: C-F Bond activation at Ni(0) and simple reactions of square planar Ni(II) fluoride complexes.
• Authors of publication: Burling, Suzanne; Elliott, Paul I. P.; Jasim, Naser A.; Lindup, Richard J.; McKenna, Jennifer; Perutz, Robin N.; Archibald, Stephen J.; Whitwood, Adrian C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 22
• Pages of publication: 3686 - 3695
• a: 10.7713 ± 0.0007 Å
• b: 13.1418 ± 0.0009 Å
• c: 16.9266 ± 0.0012 Å
• α: 90°
• β: 92.929 ± 0.002°
• γ: 90°
• Cell volume: 2392.9 ± 0.3 ų
• Cell temperature: 115 ± 2 K
• Ambient diffraction temperature: 115 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0327
• Residual factor for significantly intense reflections: 0.0275
• Weighted residual factors for significantly intense reflections: 0.0694
• Weighted residual factors for all reflections included in the refinement: 0.0721
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No