Information card for entry 7001048

Structure parameters

• Formula: C33 H47 B2 Li O2 P2
• Calculated formula: C33 H47 B2 Li O2 P2
• Title of publication: Synthesis and crystal structures of bis(diphenylphosphanyl)methanides of lithium and calcium as well as of their borane adducts
• Authors of publication: Langer, Jens; Wimmer, Katja; Görls, Helmar; Westerhausen, Matthias
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 16
• Pages of publication: 2951 - 2957
• a: 10.0747 ± 0.0008 Å
• b: 11.1578 ± 0.0007 Å
• c: 16.7869 ± 0.0013 Å
• α: 97.819 ± 0.004°
• β: 104.841 ± 0.003°
• γ: 106.881 ± 0.004°
• Cell volume: 1699.7 ± 0.2 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1241
• Residual factor for significantly intense reflections: 0.0834
• Weighted residual factors for significantly intense reflections: 0.201
• Weighted residual factors for all reflections included in the refinement: 0.2287
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No