Information card for entry 7001049

Structure parameters

• Formula: C37 H57 B2 Li O6 P2
• Calculated formula: C37 H57 B2 Li O6 P2
• Title of publication: Synthesis and crystal structures of bis(diphenylphosphanyl)methanides of lithium and calcium as well as of their borane adducts
• Authors of publication: Langer, Jens; Wimmer, Katja; Görls, Helmar; Westerhausen, Matthias
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 16
• Pages of publication: 2951 - 2957
• a: 11.25 ± 0.0002 Å
• b: 12.3814 ± 0.0002 Å
• c: 29.645 ± 0.0005 Å
• α: 86.239 ± 0.001°
• β: 81.939 ± 0.001°
• γ: 82.513 ± 0.001°
• Cell volume: 4048.91 ± 0.12 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1443
• Residual factor for significantly intense reflections: 0.0934
• Weighted residual factors for significantly intense reflections: 0.2404
• Weighted residual factors for all reflections included in the refinement: 0.2805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No