Information card for entry 7001125

Structure parameters

• Formula: C18 H54 B2 P2 Si4
• Calculated formula: C18 H54 B2 P2 Si4
• SMILES: [BH3][P]([C@H]([Si](CC[Si]([C@H]([P]([BH3])(C)C)[Si](C)(C)C)(C)C)(C)C)[Si](C)(C)C)(C)C
• Title of publication: Synthesis and structural characterisation of alkali metal complexes of heteroatom-stabilised 1,4- and 1,6-dicarbanions
• Authors of publication: Izod, Keith; Bowman, Lyndsey J.; Wills, Corinne; Clegg, William; Harrington, Ross W.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 17
• Pages of publication: 3340 - 3347
• a: 6.6106 ± 0.0001 Å
• b: 8.716 ± 0.0002 Å
• c: 13.3995 ± 0.0004 Å
• α: 81.709 ± 0.002°
• β: 86.352 ± 0.002°
• γ: 77.554 ± 0.002°
• Cell volume: 745.61 ± 0.03 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.042
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.0754
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No