Information card for entry 7001126

Structure parameters

• Formula: C34 H84 B2 K2 O4 P2 Si4
• Calculated formula: C34 H84 B2 K2 O4 P2 Si4
• Title of publication: Synthesis and structural characterisation of alkali metal complexes of heteroatom-stabilised 1,4- and 1,6-dicarbanions
• Authors of publication: Izod, Keith; Bowman, Lyndsey J.; Wills, Corinne; Clegg, William; Harrington, Ross W.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 17
• Pages of publication: 3340 - 3347
• a: 9.3401 ± 0.0009 Å
• b: 11.313 ± 0.0011 Å
• c: 13.0533 ± 0.0013 Å
• α: 78.29 ± 0.002°
• β: 76.748 ± 0.002°
• γ: 71.916 ± 0.001°
• Cell volume: 1263.2 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0989
• Weighted residual factors for all reflections included in the refinement: 0.1037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No