Information card for entry 7002270

Structure parameters

• Formula: C37 H50 Br2 N2 O Sb
• Calculated formula: C37 H50 Br2 N2 O Sb
• Title of publication: Synthesis and structures of β-dialdiminatoantimony(III) halides and β-dialdiminium hexahalogenoantimoniates
• Authors of publication: Hitchcock, Peter B.; Lappert, Michael F.; Li, Gang; Coles, Martyn P.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 37
• Pages of publication: 7820 - 7826
• a: 13.562 ± 0.0002 Å
• b: 26.3036 ± 0.0003 Å
• c: 20.9135 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7460.46 ± 0.18 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0673
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.0695
• Weighted residual factors for all reflections included in the refinement: 0.0786
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No