Information card for entry 7002271

Structure parameters

• Formula: C136 H174 I8 N8 O Sb4
• Calculated formula: C136 H164 I8 N8 O Sb4
• Title of publication: Synthesis and structures of β-dialdiminatoantimony(III) halides and β-dialdiminium hexahalogenoantimoniates
• Authors of publication: Hitchcock, Peter B.; Lappert, Michael F.; Li, Gang; Coles, Martyn P.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 37
• Pages of publication: 7820 - 7826
• a: 51.091 ± 0.0006 Å
• b: 13.1184 ± 0.0002 Å
• c: 21.2525 ± 0.0002 Å
• α: 90°
• β: 96.067 ± 0.001°
• γ: 90°
• Cell volume: 14164.3 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0953
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No