Information card for entry 7002459

Structure parameters

• Formula: C32 H35 N O3 Pd
• Calculated formula: C32 H35 N O3 Pd
• Title of publication: Synthesis and structures of complexes with axially chiral isoquinolinyl-naphtholate ligands
• Authors of publication: Howard, Ruth H.; Alonso-Moreno, Carlos; Broomfield, Lewis M.; Hughes, David L.; Wright, Joseph A.; Bochmann, Manfred
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 40
• Pages of publication: 8667 - 8682
• a: 11.2647 ± 0.0013 Å
• b: 26.934 ± 0.003 Å
• c: 11.8122 ± 0.0014 Å
• α: 90°
• β: 112.275 ± 0.011°
• γ: 90°
• Cell volume: 3316.4 ± 0.7 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2249
• Residual factor for significantly intense reflections: 0.0832
• Weighted residual factors for significantly intense reflections: 0.1538
• Weighted residual factors for all reflections included in the refinement: 0.1884
• Goodness-of-fit parameter for all reflections included in the refinement: 0.93
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No