Information card for entry 7002628

Structure parameters

• Formula: C102 H89 Ag3 Cl I2 N3 O4 P6
• Calculated formula: C96 H75 Ag3 Cl I2 N3 O4 P6
• Title of publication: Synthesis and reactivity of diphosphine metal complexes bearing peripheral ketenimine functionalities
• Authors of publication: Ruiz, Javier; Gonzalo, Marta P.; Vivanco, Marilín; Quesada, Roberto; Mosquera, Marta E. G.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 9280
• a: 12.8216 ± 0.0005 Å
• b: 19.232 ± 0.0007 Å
• c: 20.9922 ± 0.0008 Å
• α: 110.96 ± 0.002°
• β: 104.228 ± 0.002°
• γ: 92.629 ± 0.003°
• Cell volume: 4634.1 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.066
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1537
• Weighted residual factors for all reflections included in the refinement: 0.1654
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No